Choline in Infant Formula and Adult/Pediatric Nutritional Formula by Ultra High-Performance Liquid Chromatography/Tandem Mass Spectrometry: AOAC First Action 2012.18-Reference-Cited by-同舟云学术

Choline in Infant Formula and Adult/Pediatric Nutritional Formula by Ultra High-Performance Liquid Chromatography/Tandem Mass Spectrometry: AOAC First Action 2012.18

Published:2013-11-01 Issue:6 Volume:96 Page:1396-1399
ISSN:1060-3271
Container-title:Journal of AOAC INTERNATIONAL
language:en
Short-container-title:

Author:

Martin Frederic¹,Gimenez Catherine¹,Fontannaz Patric¹,Kilinc Tamara¹,Campos-Giménez Esther¹,Dowell Dawn²

Affiliation:

1. Nestlé Research Center, Vers-chez-les-Blanc, 1000 Lausanne 26, Switzerland

2. AOAC INTERNATIONAL, 481 N. Frederick Ave, Suite 500, Gaithersburg, MD 20877-2417

Abstract

Abstract The method described below is for the determination of choline in infant formula and adult/pediatric nutritional formula by ultra high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS). The single-laboratory validation data were submitted to the Stakeholder Panel on Infant Formula and Adult Nutritionals (SPIFAN) Expert Review Panel (ERP) for review at the AOAC INTERNATIONAL Annual Meeting held September 30 to October 3, 2012 in Las Vegas, NV. The ERP determined that the data reviewed met the standard method performance requirements set by SPIFAN, and the method was approved as AOAC Official First Action. The analytical range was found to be between 0.16 and 3.2 μg/mL. The recovery rates were within 80–120% at 50 and 100% of native levels for all samples. Repeatability precision (RSDr) was <3%, with intermediate reproducibility (RSDir) no higher than 4%.

Publisher

Oxford University Press (OUP)

Subject

Pharmacology,Agronomy and Crop Science,Environmental Chemistry,Food Science,Analytical Chemistry

Link

http://academic.oup.com/jaoac/article-pdf/96/6/1396/32423817/jaoac1396.pdf

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