Mechanochemical Synthesis and Reactivity of a Stable Nickel Borohydride

Author:

Raje Sakthi1ORCID,Mani Kalaikodikumaran1ORCID,Dinesh Shruthi1,Yadav Archana1,Chahal Manoj1ORCID,Butcher Ray J.2ORCID,Angamuthu Raja13ORCID

Affiliation:

1. Department of Chemistry Indian Institute of Technology Kanpur Kanpur 208016 India

2. Department of Chemistry Howard University Washington D.C. 20059 USA

3. Department of Sustainable Energy Engineering Indian Institute of Technology Kanpur Kanpur 208016 India

Abstract

AbstractWe report the solvent‐assisted mechanochemically synthesised mononuclear Ni(II) borohydride complex supported by a macrocyclic tetradentate ligand. It was characterised as stable high‐spin [(LMe)Ni(η2‐BH4)]+ cation in solid‐state and in solution by various physicochemical methods and capable of transferring hydride. The stoichiometric reactivity of [(LMe)Ni(η2‐BH4)]+ cation was examined with trityl cation, alkyl halide, disulphide, thiol, carboxylic acid and enol at room temperature.

Funder

Indian Institute of Technology Kanpur

Science and Engineering Research Board

Publisher

Wiley

Subject

Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry,Drug Discovery,Biochemistry,Catalysis

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