Electrochemical Cascade Annulation for the Synthesis of 3‐Sulfanylquinoline Derivatives Under Mild Conditions

Author:

Li Ke1,Guo Ming‐Zhong1,Chen Zhuo1,Li Hao‐Ran1,Guo Weisi1,Li Ming1,Zhang Lin‐Bao1

Affiliation:

1. State Key Laboratory Base of Eco‐Chemical Engineering, College of Chemistry and Molecular Engineering Qingdao University of Science & Technology Qingdao Shandong 266042 China

Abstract

Comprehensive SummaryAn efficient electrochemical approach has been developed for the construction of 3‐sulfanylquinoline derivatives by treating phenylethynylbenzoxazinanones with disulfides in an undivided cell. The protocol provided a convenient route to functionalized quinolines with good functional group tolerance. Moreover, it does not require any metal catalysts or additives, furnishing a series of biological quinolines in moderate to good yields.

Funder

National Natural Science Foundation of China

Publisher

Wiley

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