One‐Step Synthesis of Pseudo‐Boehmite by Carbonation in a Microchannel Reactor

Author:

Zhang Xing12,Chen Jiayu2,Jiang Tao2,Fu Jianmin2,Wu Xuantao2,Wang Hui23,Sun Yuhan23

Affiliation:

1. ShanghaiTech University School of Physical Science and Technology 201210 Shanghai China

2. Shanghai Institute of Cleantech Innovation 201616 Shanghai China

3. ShanghaiTech University Institute of Carbon Neutrality 201210 Shanghai China

Abstract

AbstractPseudo‐boehmite with a high specific surface area and large pore volume was continuously synthesized in a microchannel reactor using the carbonation method. The effects of the microchannel on the prepared pseudo‐boehmite, strongly present in gas‐liquid mixing efficiency, were studied. In time scale, the crystallinity of pseudo‐boehmite in the microchannel, without the aging process of high‐temperature stirring, reaches the standard of industrial products. Besides, the fluid and mass transfer effect of the gas‐liquid mixing process in the microreactor was simulated under experimental conditions in computational fluid dynamics. The result illustrated the base‐liquid surround by the acid‐gas model in the microreactor, which is significantly different from the batch reactor.

Publisher

Wiley

Subject

Industrial and Manufacturing Engineering,General Chemical Engineering,General Chemistry

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