Enhancing Mechanical Properties of Carbon–Silicon Steel through Two‐Stage Quenching and Partitioning with Bainitic Transformation: Ultimate Tensile Strength of 1875 MPa and Total Elongation of 8.03%

Author:

Masoumi Mohammad1ORCID,Centeno Dany2,Tressia Gustavo3,Loureiro Rodrigo C. P.4,Carvalho Felipe M.2,Marquez‐Rossy Andres5,Poplawsky Jonathan D.6ORCID,Ariza‐Echeverri Edwan Anderson7ORCID

Affiliation:

1. Engineering Center, Modelling and Applied Social Science (CECS) Federal University of ABC (UFABC) Santo André SP 09210‐580 Brazil

2. Metallurgical Processes Laboratory Institute for Technological Research Av. Prof. Almeida Prado São Paulo 05508‐080 Brazil

3. Vale Technological Institute Juscelino Kubitschek Avenue 3, Bauxita Ouro Preto MG 35400‐000 Brazil

4. Department of Metallurgical and Materials Engineering Federal University of Ceará Fortaleza CE 60445‐554 Brazil

5. Materials Science & Technology Division Oak Ridge National Laboratory Oak Ridge 37831 TN USA

6. Center for Nanophase Materials Sciences Oak Ridge National Laboratory Oak Ridge 37831 TN USA

7. Grupo de Nuevos Materiales Facultad de Ingeniería Universidad del Magdalena Santa Marta 470004 Colombia

Abstract

To achieve the desired microstructural properties, the ongoing development and innovation in new structural steels require novel thermal processing. This study aims to improve the mechanical properties of a commercial spring carbon–silicon steel by tailoring its microstructure through a process involving quenching and partitioning (Q&P) followed by bainitic transformation. A two‐stage Q&P process is proposed to generate a nanoscale dispersion of stable retained austenite and carbides within the tempered martensite and bainite microstructure. The resulting tensile properties demonstrate a yield strength of 1280 MPa, an ultimate tensile strength of 1875 MPa, and a total elongation of 8.03%. These values surpass those of conventional spring 9254 steel, highlighting the effectiveness of the thermal treatment design. Microstructure analysis reveals the presence of tempered martensite, bainite sheaves, nanoscale carbides, and aggregates of retained austenite. Moreover, the resulting body‐centered cubic matrix exhibits minimal lattice tetragonality of ≈1.0051, coupled with stable retained austenite featuring a carbon concentration of ≈3.42 ± 0.5 wt%, resulting in outstanding strength–ductility properties. These findings indicate that the proposed two‐stage Q&P process, followed by bainitic transformation, significantly enhances the mechanical properties of carbon–silicon steels, making it a promising candidate for high‐performance spring applications.

Publisher

Wiley

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