CAT on MOUSE: Control and automation of temperature for single‐sided NMR instruments such as NMR‐MOUSE

Author:

Mailhiot Sarah1,Mankinen Otto1ORCID,Li Jing12,Kharbanda Yashu13,Telkki Ville‐Veikko1ORCID,Urbańczyk Mateusz4ORCID

Affiliation:

1. NMR Research Unit University of Oulu Oulu Finland

2. NIMBE, CEA, CNRS, Université de Paris Saclay, CEA Saclay Gif‐sur‐Yvette France

3. Laboratoire Navier (Ecole des Ponts ParisTech—Université Gustave Eiffel) Champs‐sur‐Marne France

4. Institute of Physical Chemistry Polish Academy of Sciences Warsaw Poland

Abstract

AbstractTemperature‐dependent experiments are a rapidly growing area of interest for low‐field NMR. In this work, we present a new device for wide‐range temperature control for single‐sided NMR instruments. The presented device, called CAT, is simple to build, inexpensive, and easy to modify to accommodate different samples. We present the capabilities of the device using a freezing temperature study of acetic acid/water mixtures. Additionally, we present the stability of the device over long measurement times. We believe that by introducing such a device with an open‐source design, we allow researchers to use it in a wide range of applications and to fully incorporate variable‐temperature studies in the world of single‐sided instruments.

Funder

Academy of Finland

H2020 European Research Council

KAUTE-Säätiö

Narodowym Centrum Nauki

Oulun Yliopisto

Publisher

Wiley

Subject

General Materials Science,General Chemistry

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