Affiliation:
1. Dental Medicine Study Program, Faculty of Medicine Universitas Jendral Soedirman Purwokerto Indonesia
2. Materials Science and Engineering Research Group, Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Bandung Indonesia
3. Research Center for Nanoscience and Nanotechnology Institut Teknologi Bandung Bandung Indonesia
4. Engineering Physics Research Group, Faculty of Industrial Technology Institut Teknologi Bandung Bandung Indonesia
Abstract
ABSTRACTThis study aimed to evaluate the effect of incorporating nanocrystalline cellulose (NCC) sourced from rice husk on the mechanical properties of a commercial glass ionomer cement (GIC). NCC was isolated through acid hydrolysis, and its crystallinity, chemical structure, and morphology were characterized through x‐ray diffractometry, Fourier‐transform infrared spectroscopy, and transmission electron microscopy, respectively. Various concentrations of NCC (0%, 0.5%, 1%, and 1.5%) were added to reinforce the GIC matrix. Mechanical tests including compressive strength, flexural strength, hardness, and shear bond strength were conducted on the modified GIC samples. The addition of NCC resulted in increased hardness and shear bond strength values, with 1% NCC showing the highest values compared to other concentrations. However, there was no significant improvement observed in the compressive and flexural strength of the modified GIC. Failure mode test revealed a reduction in adhesive failure with the addition of NCC. Incorporating small amounts of NCC (0.5%–1%) suggests a promising and affordable modification of GIC restorative material using biomass residue, resulting in improved mechanical properties.