Rapid and mild silylation ofβ-amino alcohols at room temperature mediated byN-methylimidazole for enhanced detectability by gas chromatography/electron ionization mass spectrometry
Author:
Affiliation:
1. Physical and Life Sciences Directorate; Lawrence Livermore National Laboratory; Livermore CA 94550 USA
2. Forensic Science Center; Lawrence Livermore National Laboratory; Livermore CA 94550 USA
Publisher
Wiley
Subject
Organic Chemistry,Spectroscopy,Analytical Chemistry
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2. Review: Derivatization in mass spectrometry - 1. Silylation;Halket;Eur. J. Mass Spectrom.,2003
3. A new silylation reagent for amino acids bis(trimethylsilyl)trifluoroacetamide (BSTFA);Stalling;Biochem. Biophys. Res. Commun.,1968
4. Conversion of steroids to trimethylsilyl derivatives for gas phase analytical studies;Chambaz;Anal. Biochem.,1969
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