A simple criterion for gas chromatography/mass spectrometric analysis of thermally unstable compounds, and reassessment of the by-products of alkyl diazoacetate synthesis

Author:

Kornilova Tatiana A.1,Ukolov Anton I.1,Kostikov Rafael R.1,Zenkevich Igor G.1

Affiliation:

1. Department of Chemistry, St. Petersburg State University; Universitetskii prosp. 26; St. Petersburg 198504 Russia

Publisher

Wiley

Subject

Organic Chemistry,Spectroscopy,Analytical Chemistry

Reference15 articles.

1. Use of retention data as the first step in the identification of cyclic organic peroxides in temperature-programmed gas chromatography;Barreto;Chromatographia,2006

2. Trace level detection and quantitation of ethyl diazoacetate by reversed-phase high performance liquid chromatography and UV detection;Axe;J. Pharm. Biomed. Anal.,2006

3. The NIST 11 Mass Spectral Library (NIST11/2011/EPA/NIH) Software/Data Version (NIST08); NIST Standard Reference Database, Number 69, National Institute of Standards and Technology 2011 http://webbook.nist.gov

4. Mass spectra and appearance potentials of diazirine and diazomethane;Paulett;J. Chem. Phys.,1963

5. Metal salt catalysed carbenoids. XVIII. The electron impact mass spectral behavior of diazocarbonyl compounds. I;Wulfman;Can. J. Chem.,1984

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