1. Department of Chemistry, University of York, Heslington, York, YO10 5DD, UK, Fax: +44‐1904‐432516
2. School of Chemistry, Newcastle University, Newcastle upon Tyne, NE1 7RU, UK
3. EPSRC National Crystallography Service, School of Chemistry, University of Southampton, Highfield, Southampton, SO17 1BJ, UK