1. Escola Politecnica, Department of Metalurgical and Materials Engineering, University of São Paulo, Av. Prof. Mello Moraes 2463, São Paulo, SP 05508‐900, Brazil, Fax: +55‐11‐3091‐5238
2. Centro Universitário da FEI, Av. Humberto A. C. Branco, 3973, São Bernardo do Campo, SP 09850‐901, Brazil
3. Instituto de Física, University of São Paulo CP 33618, São Paulo, SP 05315‐970, Brazil
4. Brazilian Synchrotron Light Laboratory, LNLS, CP 6192, Campinas, SP 13084‐971, Brazil