One‐pot green synthesis, study of fluorescence properties, and biological activity of pyrano[3,2‐c]chromenes derivatives via mesoporous materials MgO/SBA‐15

Author:

Chelihi Ahmed1,Hassaine Ridha12ORCID,Nachat Souad1,Benabdallah Mohammed1ORCID,Bendahou Karima1ORCID,Aissaoui Mohammed34ORCID,Saidj Merzouk5,Djafri Ahmed25,Boukenna Leïla26ORCID,Bouchama Abdelghani2,Choukchou‐Braham Noureddine1ORCID,Taibi Nadia27ORCID

Affiliation:

1. Laboratoire de Catalyse et Synthèse en Chimie Organique, Faculté des Sciences Université de Tlemcen Tlemcen Algeria

2. Centre de Recherche Scientifique et Technique en Analyses Physico‐chimiques CRAPC Bou‐Ismail, Tipaza Algeria

3. Biology Departement, Faculty of Sciences and Technology University of Tamanghasset Tamanghasset Algeria

4. Laboratoire Antibiotiques Antifongiques: Physicochimie, Synthèse et Activité Biologique Université de Tlemcen Tlemcen Algeria

5. Laboratory of Technology and Solid Properties, Faculty of Sciences and Technology Abdelhamid Ibn Badis University of Mostaganem Mostaganem Algeria

6. Laboratoire de Chimie Organique Appliquée, Faculté des Chimie USTHB El‐Alia, Alger Algeria

7. Laboratoire de Recherche sur Les Zones Arides (LRZA), Faculté des Sciences Biologiques (FSB) Université des Sciences et de La Technologie Houari Boumediene (USTHB) El Alia, Bab Ezzouar Algeria

Abstract

AbstractThis current work describes the preparation of MgO‐SBA‐15 catalysts by ultrasonic method, and it is characterized by the different analysis techniques of XRD, BET, SEM, and IRTF. In order to find out an application for this mesoporous material, MgO/SBA‐15 was used as a heterogeneous catalyst in the one‐pot synthesis of pyrano[3,2‐c]chromenes derivatives isolated at room temperature reaction according to green chemistry criteria. To enhance these derivatives, a spectroscopic study of molecular fluorescence properties was carried out as well as an identification analysis by nuclear magnetic resonance and FTIR was used. Furthermore, biological activity experiment is also carried out, from where the obtained test results were satisfactory for AC09, AC05, and AC10 compounds and they are checked after computation by molecular modeling.

Publisher

Wiley

Subject

Organic Chemistry

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