Synthesis of colorless polyimides derived from benzimidazole diamines with bis‐amide structures

Author:

Zhang Hao1,Guo Feng1,Xu Ke1,Wang Mengxia1,Chen Chunhai1,Qian Guangtao2,Liu Gang1ORCID,Deng Zhiqing3

Affiliation:

1. State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, Center for Advanced Low‐dimension Materials, College of Material Science and Engineering Donghua University Shanghai People's Republic of China

2. Center for Civil Aviation Composites Donghua University Shanghai People's Republic of China

3. Shanghai Institute of Precision Measurement and Test Shanghai China

Abstract

AbstractTo make the colorless polyimides (CPIs) suitable for the application of flexible display technology, the polyimide (PI) films need to have both good optical properties and thermal properties. To get the wanted properties, 2‐(2‐methyl‐4‐(2‐methyl‐4‐aminobenzamido)phenyl)‐5‐(2‐methyl‐4‐aminobenzamido)‐N‐phenylbenzimidazol (5a) and 2‐(2‐methyl‐4‐(2‐trifluoromethyl‐4‐aminobenzamido)phenyl)‐5‐(2‐trifluoromethyl‐4‐aminobenzamido)‐N‐phenylbenzimidazol (5b) were synthesized, which both contained benzimidazole and bis‐amide structures. Two kinds of PI films were polymerized with cyclobutane‐1,2,3,4‐tetracarboxylic dianhydride (CBDA). With the contribution of side groups (CH3 or CF3), the resulting PI films presented relatively superior optical properties (transmittance at 400 nm was 59% and 68% respectively) and low coefficient of thermal expansion (CTE = 22 and 25 ppm K−1). These good properties suggest that these PI films have the potential for flexible display usage.

Funder

Fundamental Research Funds for the Central Universities

Publisher

Wiley

同舟云学术

1.学者识别学者识别

2.学术分析学术分析

3.人才评估人才评估

"同舟云学术"是以全球学者为主线,采集、加工和组织学术论文而形成的新型学术文献查询和分析系统,可以对全球学者进行文献检索和人才价值评估。用户可以通过关注某些学科领域的顶尖人物而持续追踪该领域的学科进展和研究前沿。经过近期的数据扩容,当前同舟云学术共收录了国内外主流学术期刊6万余种,收集的期刊论文及会议论文总量共计约1.5亿篇,并以每天添加12000余篇中外论文的速度递增。我们也可以为用户提供个性化、定制化的学者数据。欢迎来电咨询!咨询电话:010-8811{复制后删除}0370

www.globalauthorid.com

TOP

Copyright © 2019-2024 北京同舟云网络信息技术有限公司
京公网安备11010802033243号  京ICP备18003416号-3