1. State Key Laboratory of Silicon Materials Department of Polymer Science and Engineering; Zhejiang University; Hangzhou 310027 P. R. China
2. Department of Chemistry; Zhejiang University; Hangzhou 310027 P. R. China
3. Surface and Microbeam Analysis; Materials Analysis Station; National Institute for Materials Science; Tsukuba 305-0047 Japan
4. Nano Characterization Unit; National Institute for Materials Science; Tsukuba 305-0047 Japan