The insertion and extrusion of heterosulfur bridges.XIII.Syntheses and structural studies of nitrophenanthro[4,5-bcd]thiophenes

Author:

Klemm L. H.,Tsuchiya Reiko,Wong Eric K. L.,Stevens Michael P.,Lu Jennifer J.,Klopfenstein C. E.

Publisher

Wiley

Subject

Organic Chemistry

Reference19 articles.

1. Condensed thiophenes from sulfur bridging. I. Phenanthro[4,5-bcd]thiophene

2. The insertion and extrusion of heterosulfur bridges. III. A useful chemical-chromatographic separation procedure

3. It is suggested that the acetonitrile used in our original studies contained amine impurities [9] which caused the reaction to proceed [10]. Later, unsuccessful attempts to reproduce the original reaction were made with acetonitrile with a higher degree of purity.

4. G. Barbieri, M. Cinquini, S. Colonna, and F. Montanari, [J. Chem. Soc., (C), 659 (1968)] recommend use of aqueous pyridine for oxidation of sulfides to sulfoxides by means of iodobenzene dichloride.

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