N‐Formylation of amines using a domestic microwave oven and bioactivities of some N‐formamides

Author:

Mai Nguyen Thi Ngoc1,Van Dat Nguyen2ORCID,Huan Trinh Thi1,Hoan Duong Quoc2

Affiliation:

1. Department of Science Hong Duc University 565 Quang Trung, Thanh Hoa City, Nghe An 43000 Viet Nam

2. Department of Chemistry Hanoi National University of Education 136 Xuan Thuy, Cau Giay Hanoi 10000 Viet Nam

Abstract

AbstractA reasonable and chemoselective approach for N‐formylation of various amines with N,N‐dimethylformamide in presence of acetic acid has been improved under irradiation of a domestic microwave oven. The method was found to be compatible with primary, secondary, aromatic and aliphatic amines with electron withdrawing and electron donating groups as well but did not support to form N‐formate derivatives. N‐formamides 1, 2, and 3 did not exhibit antibacterial activity on Gram(+), Gram(‐) and fungi but compounds 1, 2, 18 and 19 showed weak antioxidant activity with SC: 36.8 %, 38.3 %, 45.7 %, respectively. Compound 18 exhibited antioxidant activity with SC50: 47.2 μg/mL.

Publisher

Wiley

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