Affiliation:
1. Electronic Materials Research Laboratory, Department of Physics, Mar Ivanios College, Thiruvananthapuram, Kerala 695015, India
Abstract
We investigated the chemical reactivity and percolation characteristics of insulating nanocrystalline YBa2ZrO5.5 prepared by modified combustion route and the YBa2Cu3O7−δ superconductor composite system. Structural analysis was done by using X-ray diffraction technique, surface morphology of the samples was studied using scanning electron microscopy, and electrical transport measurements like critical transition temperatures (Tc) and self-field transport critical current (Jc) were done by using standard four-probe technique. It is found that, in YBa2Cu3O7−δ-nano-YBa2ZrO5.5 composite system, the superconductor and insulator materials coexist as separate phases without any noticeable chemical reaction even after sintering at high temperatures. Furthermore, percolation threshold and critical exponent are found to be VC=0.3, t=1.68, and u=2.7. And the analysis of the current flow in the polycrystalline samples reveals weak link behavior in the majority of grain connections.
Funder
Council for Scientific and Industrial Research, South Africa
Subject
General Earth and Planetary Sciences,General Engineering,General Environmental Science