Characteristics of Carbon Nanospheres Prepared from Locally Deoiled Asphalt

Author:

Ibrahim Mohammed Mohammed1,Ismaeel Ibrahim Raheek1ORCID,Mahmoud Luma Hussein1,Zablouk Mumtaz Abdulahad1,Manweel Neeran1,Mahmoud Abeer1

Affiliation:

1. Chemical Engineering Department, University of Technology, Baghdad, Iraq

Abstract

Iraqi deoil asphalt as a source of carbon is used to prepare the carbon nanospheres (CNS) by chemical vapor deposition (CVD) method. Asphalt after further chemical treatment to remove aromatic oil and impurities was crushed, weighted and evaporated under inert atmosphere using argon. The vapor/argon mixture was allowed to pass through high temperature zone 900°C in quartz tube over CO/Al2O3catalyst material. The carbon precipitated from the decomposition of asphalt vapor was collected and identified using atomic force microscope (AFM), scanning electron microscope (SEM), X-ray diffractometer (XRD), BET surface area technique and atomic force microscope. A sphere shape of carbon (94%) with nanosize and diameter less than 100 nm with surface area of 360 m2/g has been obtained.

Publisher

Hindawi Limited

Subject

General Engineering,General Materials Science

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1. Preparation of carbon materials by vapor deposition with Fe3+-Modified nickel foam from biomass pyrolysis gas;Journal of the Energy Institute;2024-10

2. “Synthesis of carbon nanomaterials by chemical vapor deposition method using green chemistry principles”;Handbook of Greener Synthesis of Nanomaterials and Compounds;2021

3. One-step synthesis and characterization of carbon nanospheres via natural gas condensate pyrolysis;Fullerenes, Nanotubes and Carbon Nanostructures;2020-04-15

4. Less-Common Carbon Nanostructures;Carbon Allotropes: Metal-Complex Chemistry, Properties and Applications;2019

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