1. Department of Physical Metallurgy, TU Clausthal, Großer Bruch 23, Clausthal-Zellerfeld D-38678, Germany
2. Institute of Geology and Paleontology, TU Clausthal, Leibnizstr. 10, Clausthal-Zellerfeld D-38678, Germany
3. joint Institute of Nuclear Research, Frank Laboratory for Neutron Physics, Dubna, Moscow Region 141980, Russia