H-ZSM-5 Zeolite Synthesis by Sourcing Silica from the Wheat Husk Ash: Characterization and Application as a Versatile Heterogeneous Catalyst in Organic Transformations including Some Multicomponent Reactions-Reference-Cited by-同舟云学术

H-ZSM-5 Zeolite Synthesis by Sourcing Silica from the Wheat Husk Ash: Characterization and Application as a Versatile Heterogeneous Catalyst in Organic Transformations including Some Multicomponent Reactions

Published:2015-01-29 Issue: Volume:2015 Page:1-14
ISSN:2314-5102
Container-title:Journal of Catalysts
language:en
Short-container-title:Journal of Catalysts

Author:

Shaikh Isak Rajjak¹²³,Shaikh Rafique Ahmed⁴,Shaikh Alamgir Abdulla²,War Javeed Ahmad⁵,Hangirgekar Shankar Poshetti⁶,Shaikh Ahmad Lalahmad⁶,Shaikh Parveen Rajjak⁷,Shaikh Rafik Rajjak⁸

Affiliation:

1. Department of Chemistry, Shri Jagdishprasad Jhabarmal Tibrewala University (JJTU), Vidyanagari, Chudela, Jhunjhunu District, Rajasthan 333 001, India

2. Post Graduate and Research Centre, Department of Chemistry, Poona College of Arts, Science and Commerce, Military Camp Area, Pune, Maharashtra 411 001, India

3. Razak Institution of Skills, Education and Research (RISER), H.Q.: 1-9-722, Shrinagar, Near Rafaiya Masjid and Hanuman Mandir, Nanded, Maharashtra 431 605, India

4. Division of Heterogeneous Catalysis, CSIR-National Chemical Laboratory (NCL), Dr. Homi Bhabha Road, Pune, Maharashtra 411 008, India

5. Department of Chemistry, Dr. Harisingh Gour Central University (DHSGCU), Sagar, Madhya Pradesh, India

6. School of Chemical Sciences, Swami Ramanand Teerth Marathwada University (SRTMU), Vishnupuri, Nanded, Maharashtra 431 601, India

7. School of Earth Sciences, Swami Ramanand Teerth Marathwada University (SRTMU), Vishnupuri, Nanded, Maharashtra 431 601, India

8. Department of Chemistry, Central University of Rajasthan (CURAJ), NH-8, Bandar Sindri, Kishangarh, Ajmer District, Rajasthan 305 801, India

Abstract

ZSM-5 zeolite was synthesized by sourcing silica from wheat husk ash and was converted into its protonated form following careful, conventionally accepted ion-exchange method and calcinations. The H-ZSM-5 zeolite (Si/Al ratio = 30) prepared was appropriately characterized by XRD, FT-IR, SEM, TEM, TG-DTA, CV, and so forth, and evaluated as recyclable catalyst in selective organic transformations including three- and four-component reactions. The catalytic activity of the zeolite sample supposedly relates to increased density of the accessible acid sites.

Publisher

Hindawi Limited

Subject

General Medicine

Link

http://downloads.hindawi.com/archive/2015/805714.pdf

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