A Novel Approach for Fabricating LaMnO3 Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques

Author:

Tran Thi Ha1,Tang Thi Trung Anh2,Pham Nguyen Hai2,Bach Thanh Cong2,Sai Cong Doanh2ORCID,Nguyen Quang Hoa2,Le Van Vu2,Nguyen Hoang Nam2ORCID,Doan Quoc Khoa3,Nguyen Trong Tam4,Le Viet Bau5,Ho Khac Hieu6,Nguyen Viet Tuyen2ORCID

Affiliation:

1. Hanoi University of Mining and Geology, Duc Thang, Tu Liem, Hanoi, Vietnam

2. VNU University of Science, Vietnam National University, 334 Nguyen Trai, Thanh Xuan, Hanoi, Vietnam

3. Quang Tri Teacher Training College, Quang Tri, Vietnam

4. Department of Physics, Faculty of Basic–Fundamental Sciences, Vietnam Maritime University, 484 Lach Tray, Le Chan, Hai Phong, Vietnam

5. Hong Duc University, 565 Quang Trung, Dong Ve, Thanh Hoa, Vietnam

6. Duy Tan University, 03 Quang Trung, Danang, Vietnam

Abstract

LaMnO3 (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000°C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/nitrogen flux ratio did not show a clear effect on the quality of thin films.

Funder

Vietnam National University

Publisher

Hindawi Limited

Subject

General Chemistry

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