Copolymerization of Tris(methoxyethoxy)vinyl Silane with N-Vinyl Pyrrolidone: Synthesis, Characterization, and Reactivity Relationships-Reference-Cited by-同舟云学术

Copolymerization of Tris(methoxyethoxy)vinyl Silane with N-Vinyl Pyrrolidone: Synthesis, Characterization, and Reactivity Relationships

Published:2015 Issue: Volume:2015 Page:1-8
ISSN:1687-9422
Container-title:International Journal of Polymer Science
language:en
Short-container-title:International Journal of Polymer Science

Author:

Hadi Mohammed Ameen¹²,Bin Ahmad Mansor¹,Shameli Kamyar³

Affiliation:

1. Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400 Serdang, Selangor, Malaysia

2. Department of Chemistry, College of Science for Women, University of Baghdad, Al Jadria, Baghdad 10071, Iraq

3. Malaysia-Japan International Institute of Technology (MJIIT), Universiti Teknologi Malaysia, Jalan Sultan Yahya Petra (Jalan Semarak), 54100 Kuala Lumpur, Malaysia

Abstract

Copolymer of tris(methoxyethoxy)vinyl silane (TMEVS) with N-vinyl pyrrolidone (NVP) was synthesized by free radical polymerization in dry benzene at 70°C using benzoyl peroxide (BPO) as initiator. The copolymer was characterized by viscometer, FTIR, and1H-NMR and its thermal properties were studied by DSC and TGA. The copolymer composition was determined by elemental analysis. The monomer reactivity ratios were calculated by linearization methods proposed by Fineman-Ross and Kelen-Tudos. The intersection method was proposed by Mayo-Lewis and nonlinear method was proposed by curve-fitting procedure. The microstructure of copolymer and sequence distribution of monomers in the copolymer were calculated by statistical method.

Publisher

Hindawi Limited

Subject

Polymers and Plastics

Link

http://downloads.hindawi.com/journals/ijps/2015/219898.pdf

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2. Functional Block Copolymers: Nanostructured Materials with Emerging Applications

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