Effects of Different Polishing Systems on Surface Roughness and Crystal Structure of Zirconia

Abstract

Objective. Intraoral polishing systems have become an alternative method for reglazing, which is important to prevent or minimize rapid wear of the opposing teeth. To assess the influence of different polishing systems and duration on surface roughness and crystal structure of zirconia was compared, contributing to the preparation and effect improvement of clinical zirconia restorations. Methods. Forty-eight zirconia specimens with equal size were fabricated by cutting and sintering zirconia discs. Then X-ray diffractometer (XRD) was adopted for examination of the specimens. Six specimens were selected as the grinding-polishing group (GL) after polishing, grinding, and glazing. Then six specimens were randomly selected from the remaining specimens as the grinding-unpolished group (GR) after surface conditioning by dental diamond burs. Subsequently, based on different polishing systems and duration, the rest of specimens were divided into following groups ( $n=6$ ): Youdent-20s group (Y20), Youdent-40s group (Y40), Youdent-60s group (Y60), Toboom-20s group (T20), Toboom-40s group (T40), and Toboom-60s group (T60). Additionally, a contour graph was applied for assessing the surface roughness of zirconia, scanning electron microscope (SEM) for observing surface topography, and X-ray diffraction analysis (XRD) for determining crystal structure of zirconia. Results. The GR group had the highest roughness, and the roughness of the specimens polished for 20 s with different polishing systems was significantly higher than those polished for 40 s and 60 s with the same polishing systems. There were no significant difference between the Y20 and T20 groups, while the roughness of the specimens in both Y40 and Y60 groups was significantly higher than that of the T40 and T60 groups. And with the increasing polishing duration, the surface morphology of the specimen was gradually smooth and the morphology was gradually regular. Besides, the surface scratches of the T group were shallower than that of the Y group at the same polishing duration. The peak value of XRD profile of the specimen after grinding and polishing process was consistent with the baseline pattern of that the original specimen. Conclusion. Glazing can reduce the surface roughness of the specimens. Besides, the polishing effect of Toboom (TOB) system ( $\text{polishing}\text{duration}=60\text{s}$ ) is the best. And different polishing durations of TOB system have no significant effect on the crystal surface structure of the specimen.