An Improved And Suitable Method For Large Scale Produdcion Of Α-Monochlorocyclodecanone

Author:

Ou Wenhua1,Wang Ruolin1,Liu Ruonan1,Huang Hong2

Affiliation:

1. School of Perfume and Aroma Technology, Shanghai Institute of Technology, Shanghai, 200235, China

2. College of Marine Ecology and Environment, Shanghai Ocean University, Shanghai 201306, China

Abstract

: α-Monochlorocyclododecanone was synthesized from cyclododecane and 1,3-Dichloro-5,5-dimethylhydantoin (DCDMH) catalyzed with silica gel in MeOH. The product was obtained by crystallization with nearly 85% yield. The presented method used cheap raw materials, mild reaction conditions, simple separation method and environment-friendly process. Additionally, the current synthesis provided an ideal approach for large-scale production.

Publisher

Bentham Science Publishers Ltd.

Subject

Organic Chemistry,Biochemistry

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