Preparation and Characterization of Nickle-based Nanocatalyst for the Regioselective Synthesis Triazole Derivatives and Antimicrobial Study

Author:

Heidari Nadia1,Albadi Jalal1,Hemmati Zahra2,Jalali Mehdi3

Affiliation:

1. Department of Chemistry, College of Science, Shahrekord University, Shahrekord, Iran

2. Department of Pathobiology, School of Veterinary Medicine, Shahrekord University, Shahrekord, Iran

3. National Petrochemical Company, Petrochemical Research and Technology Company, Tehran, Iran

Abstract

Abstract: In this research, poly (4-vinyl pyridine)-supported nickel oxide nanoparticles (P4VP-NiO nanocatalyst) as an efficient recyclable catalyst have been prepared and used for the regioselective synthesis of triazole derivatives. The nanocatalyst we characterized by Fourier-transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), x-ray diffraction (XRD), thermogravimetric analysis (TGA), inductively coupled plasma (ICP), and brunauer-emmett-teller (BET) surface area analysis. The most important advantages of using poly (4-vinylpyridine)-nickel oxide nanocatalysts in these reactions are the short reaction time, cost-effectiveness, easy recycling of the catalyst, and high yield of the product. Also, the antimicrobial properties of the new triazole derivatives have been studied.

Publisher

Bentham Science Publishers Ltd.

Subject

Organic Chemistry,Biochemistry

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