The Validation Analysis Methodology to Determine the Cadmium, Indium and Impurities Concentration in Nuclear Grade Silver-indium-cadmium Alloys-Reference-Cited by-同舟云学术

The Validation Analysis Methodology to Determine the Cadmium, Indium and Impurities Concentration in Nuclear Grade Silver-indium-cadmium Alloys

Published:2022-10-29 Issue:3A Volume:10 Page:
ISSN:2319-0612
Container-title:Brazilian Journal of Radiation Sciences
language:
Short-container-title:Braz. J. Rad. Sci.

Author:

Guilherme Costa de Oliveira

Abstract

This work aims optimized to set up and an analytical method for a reliable determination of silver-indium-cadmium alloy constituents and their impurities through the use of ICP OES (Inductively coupled plasma optical emission spectrometer). It has greater precision, accuracy, and sensitivity when compared to the traditional methodology. The validation process was carried out according to INMETRO’s (Instituto Nacional de Metrologia, Qualidade e Tecnologia) Analytical Method Validation Guidance.

Publisher

Sociedade Brasilieira de Protecao Radiologica - SBPR

Subject

General Medicine

Reference11 articles.

1. W. K. ANDERSON, J. S. THEILACKER, Neutron Absorber Materials for Reactor Control, Naval Reactors, Division of Reactor Development, US Atomic Energy Commission, v. 7, p. 01-39, 1962.

2. Experiments on silver-indium-cadmium control rod failure during severe nuclear accidents

3. M. CASTANHEIRA, L. TERREMOTO, J. SILVA, C. ZEITUNI, Análise da degradação de barras absorvedoras de nêutrons de Ag-In-Cd. Parte 1: Depleção da liga, efetividade de absorção de nêutrons e propriedades mecânicas, In: INTERNATIONAL NUCLEAR ATLANTIC CONFERENCE, 2002, Rio de Janeiro. 2002. p. 11-16.

4. American Society For Testingand Materials – ASTM C752 –13. Specification for Nuclear-Grade Silver-Indium-Cádmium Alloy, 2016.

5. American Society For Testingand Materials – ASTM C760 –90. Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys, 2015.