Indentation‐induced ductile behavior of glass–ceramics involving layered aluminosilicates

Author:

Maeda Kei1ORCID,Okuma Gaku2ORCID,Yoshida Satoshi3ORCID,Wakai Fumihiro2,Takeuchi Akihisa4,Uesugi Masayuki4,Yanagioka Shun1,Matsunuma Shun1,Machida Shingo1ORCID,Yasumori Atsuo1

Affiliation:

1. Department of Materials Science and Technology Tokyo University of Science Tokyo Japan

2. Research Center for Structural Materials National Institute for Materials Science Tsukuba Japan

3. AGC Inc. Yokohama Technical Center Yokohama Japan

4. Japan Synchrotron Radiation Research Institute Sayo Japan

Abstract

AbstractContact damage in materials is critical in engineering applications because it influences mechanical resistance, such as wear, erosion, and impact failure. Indentation tests were performed using a tungsten carbide ball indenter (Hertzian contact) on the surfaces of glass–ceramics containing hexagonal CaAl2Si2O8 or mica crystals (fluorophlogopite), both of which have a layered structure. The stress–strain relation and the permanent deformation on the surface, as well as the observation of the microcrack zone by X‐ray computed tomography using synchrotron radiation, revealed that the glass–ceramic with hexagonal CaAl2Si2O8 showed ductility similar to the quasi‐plastic behavior previously observed in the mica glass–ceramic. The yield stresses of the glass–ceramics were estimated from the stress deviating from the stress–strain relation assuming complete elastic response between the ball and the sample. The ratio of the yield stress to Young modulus (Y/E) of the glass–ceramic with hexagonal CaAl2Si2O8 was determined to be higher than that of the mica glass–ceramic.

Publisher

Wiley

Subject

Materials Chemistry,Ceramics and Composites

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