The effect of chemical vapor infiltration process parameters on flexural strength of porous α‐SiC: a numerical model

Author:

Marziale Joseph J.1,Sun Jason1,Walker Eric A.1,Chen Yu1,Salac David1,Chen James1ORCID

Affiliation:

1. Department of Mechanical and Aerospace Engineering The State University of New York at Buffalo Buffalo New York USA

Abstract

AbstractThe flexural strength variability of α‐ based ceramics at elevated temperatures creates the need for an Integrated Computational Materials Engineering (ICME) framework that relates the strength of a specimen directly to its manufacturing process. To create this ICME framework, a model must first be developed which establishes a relationship between the chemical vapor infiltration (CVI) process and parameters, the resulting mesoscale pores, and the overall macroscale flexural strength. Here, a nonlinear single‐pore model of CVI is developed used in conjunction with a four‐way coupled thermo‐mechanical damage model. The individual components of the model are tested and a sample system under a four‐point bending test is explored. Results indicate that specimens with an initial porosity greater than 30% require temperatures below 1273 K to maintain structural integrity, while those with initial porosities less than 30% are temperature‐independent, allowing for optimization of the CVI processing time without compromising strength.

Funder

Office of Naval Research

Publisher

Wiley

Subject

Materials Chemistry,Ceramics and Composites

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