1. Department of Mechanical & Marine Engineering, University of Plymouth, Drake Circus, Devon PL4 8AA, UK
2. FaME38 at ILL‐ESRF, 6 rue Jules Horowitz—BP156, 38042 Grenoble Cedex 9, France
3. Department of Mechanical Engineering, PE Technikon. Private Bag X6011, Port Elizabeth 6000, South Africa
4. Institute for Materials Research, University of Salford, Newton Building, Salford, M5 4WT, UK