Mechanical properties of 3D‐printed and milled composite resins for definitive restorations: An in vitro comparison of initial strength and fatigue behavior

Author:

Prause Elisabeth1,Malgaj Tine2ORCID,Kocjan Andraž3,Beuer Florian1,Hey Jeremias4,Jevnikar Peter2,Schmidt Franziska1

Affiliation:

1. Department of Prosthodontics Geriatric Dentistry and Craniomandibular Disorders, Charité‐Universitätsmedizin Berlin Berlin Germany

2. Department of Prosthodontics, Faculty of Medicine University of Ljubljana Ljubljana Slovenia

3. Department for Nanostructured Materials Jožef Stefan Institute Ljubljana Slovenia

4. Department of Prosthodontics School of Dental Medicine, Martin‐Luther‐University Halle Germany

Abstract

AbstractObjectiveTo evaluate the flexural strength and fatigue behavior of a novel 3D‐printed composite resin for definitive restorations.Materials and MethodsFifty disc‐shaped specimens were manufactured from each of a nanohybrid composite resin (NHC), polymer‐infiltrated ceramic network (PICN), and 3D‐printed composite resin (3D) with CAD‐CAM technology. Biaxial flexural strength (σin) (n = 30 per group) and biaxial flexural fatigue strength (σff) (n = 20 per group) were measured using piston‐on‐three‐balls method, employing a staircase approach of 105 cycles. Weibull statistics, relative‐strength degradation calculations, and fractography were performed. The results were analyzed with 1‐way ANOVA and Games‐Howell post hoc test (α = 0.05).ResultsSignificant differences in σin and σff among the groups (p < 0.001) were detected. The NHC group provided the highest mean ± standard deviation σin and σff (237.3 ± 31.6 MPa and 141.3 ± 3.8 MPa), followed by the PICN (140.3 ± 12.9 MPa and 73.5 ± 9.9 MPa) and the 3D (83.6 ± 18.5 MPa and 37.4 ± 23.8 MPa) groups. The 3D group exhibited significantly lower Weibull modulus (m = 4.7) and up to 15% higher relative strength degradation with areas of nonhomogeneous microstructure as possible fracture origins.ConclusionsThe 3D‐printed composite resin exhibited the lowest mechanical properties, where areas of nonhomogeneous microstructure developed during the mixing procedure served as potential fracture origins.Clinical SignificanceThe clinical indications of the investigated novel 3D‐printed composite resin should be limited to long‐term provisional restorations. A cautious procedure for mixing the components is crucial before the 3D‐printing process, since nonhomogeneous areas developed during the mixing could act as fracture origins.

Funder

Javna Agencija za Raziskovalno Dejavnost RS

Publisher

Wiley

Subject

General Dentistry

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