1. Univ. Grenoble Alpes; CNRS, SIMaP; F-38000 Grenoble France
2. Department of Materials Science; Technische Universität Darmstadt; Darmstadt 64287 Germany
3. Otto Schott Institute of Materials Research; Friedrich Schiller University of Jena; Jena 07743 Germany
4. Advanced Photon Source; Argonne National Laboratory; Argonne Illinois 60439
5. LCR Division; Samsung Electro-Mechanics; Suwon 443-743 South Korea
6. Univ. Grenoble Alpes; CMTC; F-38000 Grenoble France