Joining of Cf/SiC composites using AlCoCrFeNi2.1 eutectic high‐entropy alloy filler by spark plasma sintering

Author:

Wang Rongpei1ORCID,Wang Gang12,Ran Songlin3ORCID,Wang Wei3,Yang Yunlong4,Zhao Yu1,Gui Kaixuan1,He Rujie5ORCID,Tan Caiwang6

Affiliation:

1. Anhui Key Laboratory of High‐Performance Non‐Ferrous Metal Materials Anhui Polytechnic University Wuhu P. R. China

2. Key Laboratory of Additive Manufacturing (3D Printing) of Anhui Province Wuhu P. R. China

3. School of Materials Science and Engineering Anhui University of Technology Maanshan P. R. China

4. School of Civil and Environmental Engineering Nanchang Institute of Science and Technology Nanchang P. R. China

5. Institute of Advanced Structure Technology Beijing Institute of Technology Beijing P. R. China

6. State Key Laboratory of Advanced Welding and Joining Harbin Institute of Technology Harbin P. R. China

Abstract

AbstractAlCoCrFeNi2.1 eutectic high‐entropy alloy was introduced to join Cf/SiC composite by spark plasma sintering technique. The influence of holding times on microstructure, shear strength and fracture behavior of the joints was studied. When held for 7 min, the typical microstructure of the Cf/SiC‐AlCoCrFeNi2.1‐Cf/SiC joint was Cf/SiC composite → CrSi2 + FCC + Al8Cr5 + graphite → CrSi2 + FCC + Al8Cr5 → CrSi2 + FCC + Al8Cr5 + graphite → Cf/SiC composite. As the holding time extended, the Ni–Si and Fe–Si brittle phases in the joint gradually reduced, and the diffusion transition layer continued to thicken. The maximum joint strength was 23.9 MPa, which was obtained at 1450°C for 7 min. Analyzed by scanning electron microscopy and energy dispersive spectroscopy, the fracture modes of the joints joined at different holding times were all brittle fracture.

Funder

Natural Science Foundation of Anhui Province

National Natural Science Foundation of China

Publisher

Wiley

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