Mark IV "Grasshopper" grazing incidence monochromator for the Canadian Synchrotron Radiation Facility (CSRF)

Abstract

The vacuum, mechanical, and optical characteristics of a "Grasshopper" grazing incidence monochromator, for use with a synchrotron radiation source in the 30–300 eV range, is described. The monochromator is compatible with ultrahigh vacuum (≤ 5 × 10−10 Torr throughout), and the motor driven scan mechanism is linear and reliable. The monochromator has been calibrated using several known absorption edges between 36 and 102 eV and a nonlinear least squares fit to the scan equation. These same absorption edges, plus a scan over zero order, show that the present resolution of the monochromator (with 10 and 16 μm exit and entrance slits respectively) is 0.16 Å (0.06 eV at the Al L2.3 edge). With 10 μm entrance and exit slits, the resolution will be very close to the theoretical Δλ = 0.083 Å.