Author:
Georgieff K. K.,Richard Y.
Abstract
Diacetylene was prepared by the reaction of 1,4-dichloro-2-butyne with sodium hydroxide. Three modifications of procedure were tried to determine which gave the highest yield and purest product. Evidence that the by-product is 2-chloro-2-butene-3-yne is presented. Several methods for purifying the diacetylene were investigated. The ultraviolet spectrum with molar extinction coefficients is given.
Publisher
Canadian Science Publishing
Subject
Organic Chemistry,General Chemistry,Catalysis
Cited by
33 articles.
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