Abstract
The synthesis of 2,3,12,13-tetraselena[4,4]metacyclophane (1) by alkaline hydrolysis of meta-xylylene selenocyanate (3a) in 8% yield is described and is shown to have different properties to those described for 1 by Günther and Salzmann. The variable temperature pmr spectra of 1 is described as is its conversion to 2,11-diselena[3,3]metacyclophane (4) by tris(diethylamino)phosphine.
Publisher
Canadian Science Publishing
Subject
Organic Chemistry,General Chemistry,Catalysis
Cited by
21 articles.
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