Minimum Miscibility Pressure Measurement with Slim Tube Apparatus - How Unique is the Value?

Abstract

Abstract Over the years, the slim tube experiment has been the most commonly used laboratory technique for determination of minimum miscibility pressure (MMP) for designing field miscible floods. However, till now, the design of these experiments is not standardized, neither in terms of set-up nor procedure. Often, the set-up, characteristics of the slim tube coil and even the experimental procedures are left to the discretion of the experimentalist, leading to very uncertain and non-unique MMP values, to say the least. Not just the uniqueness is of great concern, but also the lack of measurement repeatability; two measurements using same fluid samples under the "same experimental conditions" may result in too different MMP values. Matching these experiments with any PVT simulation package may pose a challenge, which even if a match is achieved, may be of questionable reliability. It is on this premise that this work was based. Slim tube experiments were designed and performed to study the effects of some parameters on the uniqueness and repeatability of the MMP measurements. It was found that MMP measurements are different with different injection rates. The lowest tested rate showed slightly lower MMP and better recovery performance than the other tested rates. No clear trend was noted, however. MMP was found to be lower for the larger coil diameter of the two investigated. MMP decreased as the coil length increased. The decrease in MMP with increase in coil length followed a parabolic trend. It was, therefore, concluded that laboratory measurements of MMP using the slim tube apparatus is a function of not just the characteristics of the interacting fluids but also those of the coil used as well as the choice of injection rates. The experimental design and procedure need to be unified to produce more reliable MMP data. It is the recommendation of the authors to design the experimental injection rate based on the expected field gas injection, to use the largest coil diameter possible, and to design the coil length, based on the expected well spacing between the injector and producer.