Thermal gradients in thermal analysis experiments: Criterions to prevent inaccuracies when determining sample temperature and kinetic parameters

Author:

Sánchez-Rodríguez D.ORCID,Eloussifi H.,Farjas J.ORCID,Roura P.ORCID,Dammak M.

Funder

Spanish Programa Nacional de Materiales

Tunisian Ministry of Higher Education and Scientific Research

Publisher

Elsevier BV

Subject

Physical and Theoretical Chemistry,Condensed Matter Physics,Instrumentation

Reference48 articles.

1. A simple kinetic method for the determination of the reaction model from non-isothermal experiments;Farjas;J. Therm. Anal. Calorim.,2010

2. Methodological principles in studying chemical reaction kinetics under conditions of programmed heating;Merzhanov;Thermochim. Acta,1977

3. ICTAC kinetics committee recommendations for performing kinetic computations on thermal analysis data;Vyazovkin;Thermochim. Acta,2011

4. Test method E698, Method for Arrhenius kinetic constants for thermally unstable materials using differential scanning calorimetry and the Flynn/Wall/Ozawa method;American Society for Testing and Materials (ASTM International),2005

5. Verifying the symmetry of differential scanning calorimeters concerning heating and cooling using liquid crystal secondary temperature standards;Neuenfeld;Thermochim. Acta,2006

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