Author:
Hall H.K.,Childers Kenneth,Centeno-Hall Trevor,Contreras Cristina,Mazel Brian,Menon Hari,Nguyen Van,Robertson Jeffrey,Bates Robert
Subject
Organic Chemistry,Drug Discovery,Biochemistry
Reference10 articles.
1. Diastereoselective cyclopropanation of cyclic enones with methyl dichloroacetate anion
2. A solution containing DMF (30mL), alkene (15.85g, 149.3mmol), and methyl dichloroacetate (28.6g, 200mmol) was added to a flask containing K2CO3 (45.39g), benzyltriethylammonium chloride (1.65g, 1.49mmol), and DMF (100mL) over 3h via a dropping funnel modified with an Ace Glass Valve at 40°C. Water (200mL) was added and the solution was washed with ether (3×100mL). After drying (MgSO4), filtering, and evaporating the ether, the product was vacuum distilled.
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2 articles.
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