An easy and short preparation of pentachloroacetone by selective dechlorination of hexachloroacetone under Appel conditions
Author:
Publisher
Elsevier BV
Subject
Organic Chemistry,Drug Discovery,Biochemistry
Reference25 articles.
1. Erzeugung und [4+3]‐Cycloaddition von Oxallyl‐Zwischenstufen aus 2‐Brom‐3‐pentanon und Pentachloraceton in 2,2,3,3‐Tetrafluor‐1‐propanol
2. Improved Syntheses and Some Selective Transformations of 2,2,4,4-Tetrachloro-8-oxabicyclo[3.2.1]oct-6-en-3-ones
3. Cycloaddition of Acyclic Conjugated Dienes with a Tetrachloro-Substituted Oxyallyl Intermediate Generated from Pentachloroacetone
4. Synthetic Approaches to Hydroazulenes and Guaianes through [4 + 3] Cycloadditions of Oxyallyl Intermediates
5. A rigid GABA analog from a [4+3]-cycloaddition
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1. Reduction of Trichloromethyl togem-Dichloromethyl Group with Triphenylphosphine and Water in Ethyl Acetate;ChemistrySelect;2017-10-31
2. Chemoselective Reduction of Trichloromethyl Compounds to gem-Dichloromethyl Groups Following Appel’s Reaction Protocol;The Journal of Organic Chemistry;2016-09-26
3. Degenerate Nucleophilic Substitution in Phosphonium Salts;Journal of the American Chemical Society;2014-11-11
4. Stereoselective synthesis of α-(dichloromethyl)-amines, α-(chloromethyl)amines, and α-chloro-aziridines;RSC Advances;2014
5. Systematic survey of positive chlorine sources in the asymmetric Appel reaction: oxalyl chloride as a new phosphine activator;Tetrahedron Letters;2013-12
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