Synthesis of optically active partly gem-difluorinated allylic alcohols via [2,3]-Wittig rearrangements and lipase-catalyzed reaction
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Publisher
Elsevier BV
Subject
Organic Chemistry,Drug Discovery,Biochemistry
Reference12 articles.
1. For reviews, see: (a) Kitazume, T.; Yamazaki, T. Topics in Current Chemistry; Springer Verlag, 1997; Vol. 193, pp. 91–130.
2. (b) Percy, J. M. Top. Curr. Chem. 1997, 193, 131.
3. For [2,3]-Wittig rearrangements of difluoroallylic alkoxyacetates, see: Patel, S. T.; Percy, J. M.; Wilkes, R. D. J. Org. Chem. 1996, 61, 166.
4. For examples of the synthesis of difluorinated compounds via rearrangement reactions, see: (a) Balnaves, A. S.; Gelbrich, T.; Hursthouse, M. B.; Light, M. E.; Palmer, M. J.; Percy, J. M. J. Chem. Soc., Perkin Trans. 1 1999, 2525. (b) Ito, H.; Sato, A.; Kobayashi, T.; Taguchi, T. Chem. Commun. 1998, 2441, and references cited therein. We have synthesized many types of partly gem-difluorinated compounds via radical reaction protocol: Itoh, T.; Sakabe, K.; Kudo, K.; Ohara, H.; Takagi, Y.; Kihara, H.; Zagatti, P.; Renou, M. J. Org. Chem. 1999, 64, 252.
5. Patel. S. T.; Percy, J. M.; Wilkes, R. D. Tetrahedron 1995, 51, 9201.
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