Author:
Osorio Coralia,Duque Carmenza,Koami Takeshi,Fujimoto Yoshinori
Subject
Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry,Catalysis
Reference7 articles.
1. Osorio, C.; Duque, C.; Fujimoto, Y. Phytochemistry, in press.
2. Murata, S.; Suzuki, M.; Noyori, R. Bull. Chem. Soc. Jpn. 1982, 55, 247–254; Yasuda, M.; Ide, M.; Matsumoto, Y.; Nakata, M. Synlett 1997, 899–902. Compound 2a was prepared from TBDMS ether of geraniol (2R,3S)-oxide by a slight modification of Noyori's method (DBU was not added). This modification afforded 1-TBDMS-2-TMS ether of 2a, which after desilylation gave 2a (2R:2S, 88:12). The antipode 2b (2S:2R, 87:13) was prepared from TBDMS ether of geraniol (2S,3R)-oxide in the same manner.
3. Sharpless, K. B.; Amberg, W.; Bennani, Y. L.; Crispino, G. A.; Hartung, J.; Jeong, K.-S.; Kwong, H.-L.; Moriyama, K.; Wang, Z.-M.; Xu, D.; Zhang, X.-L. J. Org. Chem. 1992, 57, 2768–2771.
4. Ohtani, I.; Kusumi, T.; Kashman, Y.; Kakisawa, H. J. Am. Chem. Soc. 1991, 113, 4092–4096.
5. The 1H NMR spectrum of the crude tri-(R)-MTPA ester of the natural tetraol sample showed the presence of the two major constituents 5b and 5d, accompanied by the two minor ones 5a and 5c.
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