Optimization of silylation using N-methyl-N-(trimethylsilyl)-trifluoroacetamide, N,O-bis-(trimethylsilyl)-trifluoroacetamide and N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide for the determination of the estrogens estrone and 17α-ethinylestradiol by gas chromatography–mass spectrometry-Reference-Cited by-同舟云学术

Optimization of silylation using N-methyl-N-(trimethylsilyl)-trifluoroacetamide, N,O-bis-(trimethylsilyl)-trifluoroacetamide and N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide for the determination of the estrogens estrone and 17α-ethinylestradiol by gas chromatography–mass spectrometry

Published:2006-03 Issue:1 Volume:1108 Page:121-128
ISSN:0021-9673
Container-title:Journal of Chromatography A
language:en
Short-container-title:Journal of Chromatography A

Author:

Shareef Ali,Angove Michael J.,Wells John D.

Publisher

Elsevier BV

Subject

Organic Chemistry,General Medicine,Biochemistry,Analytical Chemistry

Reference25 articles.

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2. Handbook of Derivatives for Chromatography;Evershed,1993

3. Stereochemistry, Mechanism and Silicon: An Introduction to the Dynamic Stereochemistry and Reaction Mechanisms of Silicon Centers;Sommer,1965

4. Protection of hydroxyl groups as tert-butyldimethylsilyl derivatives

5. Determination of endocrine disruptors in water after derivatization with N-methyl-N-(tert.-butyldimethyltrifluoroacetamide) using gas chromatography with mass spectrometric detection

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