Author:
Raston CL,White AH,Wild SB
Abstract
The crystal structure of
the title compound has been determined by direct methods from X-ray diffraction
data and refined by least squares to a residual of 0.071 for 2647 'observed'
reflections. Crystals are monoclinic, C2/c, a
= 36.81(1), b = 11.181(2), c = 20.369(5) �, β = 95.28(3)�, Z =
32. There are four independent molecules in the asymmetric unit, all with the cis disposition of ligands (<Fe-Hg),
2.498 �; <Hg-Fe-Hg), 80.9�); in one of the molecules one of the
carbonyl sites is occupied by a more substantial moiety, possibly a result of
partial occupancy of HgCl as a result of disorder or
decomposition.
Cited by
19 articles.
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