Abstract
Treatment of
tricarbonylmyrceneiron (1) with catalytic amounts of anhydrous tetrafluoroboric
acid results in cyclization to give
tricarbonyl(3,3-dimethyl-1-vinylcyclohexene)iron (4). Protonation of (4) with
excess anhydrous tetrafluoroboric acid gives a tetracarbonylallyliron complex
(5) which can be reduced with sodium borohydride to 1-ethylidene-3,3-dimethylcyclohexane
(6).
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