Author:
Bottomley GA,Carter AM,Engelhardt LM,Lincoln FJ,Patrick JM,White AH
Abstract
The crystal structure of
the title compound, [C9H8NO]2[FeCl4]C1,
has been determined by single-crystal X-ray diffraction methods at 295 K and
refined by least squares to a residual of 0.043 for 2415 independent 'observed'
reflections. Crystals are triclinic, P1, a
14.243(5), b 10.177(3), c 7.583(3) �, α 84.71(3), β
86.96(3), γ 86.50(3�, Z 2. The organic moiety is
protonated at the nitrogen atom, with the discrete chloride ions
hydrogen-bonded in lattice tunnels; this offers a rationale for the finite but
small hydrogen chloride partial pressure at room temperature.
Cited by
19 articles.
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