Author:
Eaton PJ,Lauren DR,O'Conner AW,Weavers RT
Abstract
The saturated hydrocarbons
laurenane (3) and 1βH-laurenane (4) have been synthesized. Assignments of
their 13C n.m.r. and 1H n.m.r. spectra are reported and
used, with the aid of lanthanide shift reagents, to investigate conformational
mobility of these substituted fenestranes. Some examples of long-range 13C
n.m.r. substituent effects of the ε and ζ types have been noted.
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