Author:
Bird GJ,Collins DJ,Eastwood FW,Exner RH,Romanelli ML,Small DD
Abstract
(25R)-22αN-[15ζ,17α-2H2]Spirosol-5-en-3β-ol
([15ζ,17α-2H2]solasodine) has been synthesized
from solasodine and used to make unambiguous assignments of the resonance
signals for C13, C14, C15, C17 and C20 in the 13C N.M.R. spectrum of
solasodine. The complete assignments of the 13C N.M.R. spectra of
solasodine and some of its derivatives are based on this, on paramagnetic
broadening of signals due to C22, C23, C25 and C26, and on chemical shift
considerations.
Cited by
33 articles.
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