Abstract
Di(cyclopentadienyl)titanium(III) chloride
has been prepared in high yield by addition of tetrahydrofuran to dry mixtures
of titanium trichloride and di(cyclopentadienyl)magnesium in stoicheiometric or
excess amounts. Reaction of titanium tetrachloride with excess
di(cyclopentadienyl)magnesium also yielded (C5H5)2TiCl in moderate yield. Some properties of the
compound are given, including solid state and aqueous spectra. Magnetic
measurements show the compound to have one unpaired electron per titanium atom.
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