Author:
Raston CL,White AH,Willis AC
Abstract
The crystal structure of
the title compound, [Ni(en)3] (ClO4)2,H2O,
has been determined from single-crystal X-ray diffraction data at 295(1) K and
refined by least squares to a residual of 0.093 for 1400 'observed'
reflections. Crystals are orthorhombic, P bca, a
17.043(7), b 15.922(6), c 13.496(5) Ǻ, Z 8. The precision of the structure
determination is adversely affected by very high perchlorate thermal motion.
<Ni-N> is 2.13 Ǻ.
Cited by
11 articles.
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