Residues in apples and their packaging following fumigation with methyl bromide

Abstract

Apples (cv. Granny Smith) were fumigated with 40 g methyl bromide/m3 for 2 h at 17�C, then aerated for 2 h and stored for 10 days at 1�C as a proposed quarantine schedule for export to Japan. Residues of methyl bromide decreased from 0.1 �g/g following fumigation and cold storage to <0.002 �g/g after a further 20 days at 1�C (to simulate shipping time to Japan). Statistical analysis estimated that methyl bromide residues would decrease to 0.001 �g/g after 14.2 days storage at 1�C after fumigation. Methyl bromide residues in apple carton materials decreased to <0.01 �g/g after 7 days at 1�C, and to below the detection limit (0.002 �g/g) after 7 extra days storage at 1�C. Inorganic bromide residue after fumigation and cold storage for 30 days was 3.9 �g/g. This was less than the maximum residue limit (5 �g/g) set by the US Food and Drug Administration.